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| 气相色谱法单塔双柱双检测器测定农产品中有机氯与拟除虫菊酯类农药残留应用探索 |
| New Method with Dual Detector Single Tower Two Column Gas Chromatography for Determination of Organochlorine and Pyrethroid Pesticide Residues in Agricultural Products |
| Received:July 16, 2013 |
| DOI： |
| 中文关键词: 气相色谱法;单塔双柱双检测器;有机氯;拟除虫菊酯 |
| 英文关键词: gas chromatography;single-tower double column dual-detector;organochlorine;pyrethroid |
| 基金项目: |
| Author Name | Affiliation | | LI Xiang | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China | | HUANG Yang-cheng | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China | | WENG Chun-ying | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China | | HU Zhi-xiang | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China | | LIU Ying | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China | | WEI Jiang-feng | Liuzhou Agricultural Products Quality and Safety Testing Center, Liuzhou 545001, China |
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| 中文摘要: |
| 气相色谱经加装双ECD检测器,实现单塔双柱双检测器测定农产品中有机氯、拟除虫菊酯类农药残留,在不须关机换色谱柱情况下实现双柱定性定量分析。该方法可节约大量定性分析时间,通过百菌清、氯氟氰菊酯、三唑酮、氯氰菊酯的加标回收试验,平均回收率为95.0%～102.5%,相对标准偏差为1.88%～3.72%,方法稳定可靠。 |
| 英文摘要: |
| A new method for determination of the organochlorine,pyrethroid pesticide residues in agricultural products. was developed through installation of dual ECD detector gas chromatography,single-tower double column dual detector. This method did not have to shut down to change the column for two column qualitative and quantitative analysis. The method could save a large number of qualitative analysis for chlorothalonil,cyfluthrin,triazolam tong,cypermethrin spiked recovery experiments. The average recovery of this method was 95.0% and 102.5%,relative standard deviation was 1.88%～ 3.72%,showing this method is stable and reliable. |
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